Authors
Lucas Kinard, Kurtis Kasper, and Antonios Mikos
Summary
This protocol describes the drying of dichloromethane by a simple 10 step procedure. One can implement this protocol using common lab glass and lab equipment. First, dichloromethane is refluxed with calcium hydride to remove water. Then, dichloromethane is distilled to separate it from the byproducts of the reflux reaction. This procedure can be implemented in 1 day.Further details
The protocol was published on Protocol Exchange on 12 June 2012. To see the entire protocol, click on the source link.Advertisement
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