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Crystallization of Cryptophane-A and Cryptophane-A Derivatives with and without Encapsulated Guests

External protocol Created on 30 Apr 2014

Authors

Olena Taratula, Ivan J. Dmochowski, P. Aru Hill, and Patrick J. Carroll

Summary

Detailed protocols for crystallizing cryptophane-guest complexes are provided. Cryptophane molecular cages (cryptophane-A, also tripropargyl and triallyl derivatives) were crystallized with water, xenon, methanol, or without guest via the vapor diffusion method and with chloroform via slow evaporation. The average time required to grow cryptophane crystals is 1 week.

Further details

The protocol was published on Protocol Exchange on 4 February 2011. To see the entire protocol, click on the source link.

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