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Assays of nucleosome assembly and the inhibition of histone acetyltransferase activity. (6) Reconstitution of chromatin; (7) Analysis of nucleoproteins on an agarose gel; and (8) Purification of reconstituted chromatin on a sucrose gradient

External protocol Created on 03 May 2014

Authors

Takahito Yamasaki, Takehide Murata, Chunyuan Jin, Kohsuke Kato, Michiya Noguchi, Koji Nakade, Jianzhi Pan, Kyousuke Nagata, and Kazunari Yokoyama

Summary

Mononucleosomes can be reconstituted on 197-bp or 147-bp radiolabeled DNA fragments (see Notes 1 and 2) either by salt dialysis using purified core histones or by histone octamer transfer from donor H1-depleted chromatin. Usually, reconstitution yields naked DNA and DNA with mono-, di-, and trinucleosome cores. The efficiency of reconstitution and the number of nucleosome cores on a labeled DNA fragment can be analyzed by agarose gel electrophoresis. Reconstituted oligonucleosomes can be separated by sucrose gradient centrifugation on the basis of the number of histone octamers bound to a DNA fragment. We use 5% to 20% (w/v) linear sucrose gradients to isolate dinucleosomes from unreconstituted DNA, free histones, mono- and trinucleosomes. For a detailed introduction to assays of nucleosome assembly and the inhibition of histone acetyltransferase activity, please go here: http://www.natureprotocols.com/2007/07/30/assays_of_nucleosome_assembly.php

Further details

The protocol was published on Protocol Exchange in 2007. To see the entire protocol, click on the source link.

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