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One Heterogeneous Catalyst Drives Two Selective Fenton-like Reaction Modes for Sustainable Water Decontamination.

Created on 17 Apr 2025

Authors

Tian Yang, Min Chen, Jiejie Li, Zhiyuan Feng, Shihua Zou, Shun Mao, Ziqi Tian, Hongying Zhao

Published in

Environmental science & technology. Apr 16, 2025. Epub Apr 16, 2025.

Abstract

Heterogeneous Fenton-like reactions based on nonradical reactive oxygen species (ROS) are desirable for selective water decontamination, and different pollutants coexisting in real scenarios necessitate a rational combination of multiple ROS for efficient and sustainable decontamination. However, the general one-catalyst-for-one-ROS strategy toward selective ROS generation inevitably renders the combinational process lengthy and cost ineffective. Herein, we developed a new approach to enable the separate but selective generation of two distinct ROS in one catalyst via peroxymonosulfate activation. The unique catalyst is comprised of a graphitic layer bottom-wrapped Fe@Fe3C encapsulated inside nitrogen-doped carbon nanotubes. The Fe3C shell facilitates selective formation of surface-bound FeIV═O with up to 96.0% selectivity, and the applied electric field could switch ROS generation toward free 1O2 with 90.5% selectivity, as enabled by C atoms adjacent to graphite N. One dual-site catalyst enables both high cumulative concentration for FeIV═O and 1O2 up to 16605 and 7674 μM at 30 min, respectively. Based on such a simple electricity on/off switch mode, a tandem process operated in one unit was proposed to efficiently degrade mixed pollutants of distinct adsorption properties. This study presents a simple but very effective strategy to modulate selective ROS generation that simplifies tandem Fenton-like systems for sustainable water decontamination.

PMID:
40239063
Bibliographic data and abstract were imported from PubMed on 17 Apr 2025.

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