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Mitochondrial apoptosis and DNA intercalation synergistically driven by organotin acridine-9-carboxylate complexes potent anticancer efficacy.

Created on 29 Jul 2026

Authors

Zhijian Zhang, Zhongshan Zhou, Wujiu Jiang, Yuxing Tan

Published in

Journal of inorganic biochemistry. Volume 284. Pages 113422. Jul 27, 2026. Epub Jul 27, 2026.

Abstract

Four organotin acridine-9-carboxylate complexes (C1-C4) were successfully synthesized by the reaction of 9-acridinecarboxylic acid (YCOOH) with organotin precursors. The structures of these complexes were systematically characterized using elemental analysis, IR, NMR, X-ray single-crystal diffraction, X-ray powder diffraction and thermogravimetric analysis. Among them, the tributyltin complex C4 exhibited the most potent in vitro antiproliferative activity against HepG2, MCF-7, and NCI-H460 cancer cell lines, with IC50 values as low as 0.08 μM against HepG2 cells. Mechanistic studies identified two functional pathways: (i) DNA intercalation, as evidenced by UV-Vis, fluorescence titrations, viscosity measurements, and molecular docking, which directly disrupts DNA architecture; and (ii) mitochondria-mediated apoptosis, characterized by collapse of mitochondrial membrane potential (ΔΨm), cytochrome c (CytC) release, elevated ROS generation, upregulation of Bax and Cleaved-caspase-3, and downregulation of Bcl-2. Importantly, these two pathways act synergistically: DNA intercalation triggers early nuclear stress, which amplifies mitochondrial dysfunction and ROS burst, thereby lowering the apoptotic threshold and enhancing the overall cytotoxic efficacy. Collectively, the dual DNA-mitochondria targeting and their cooperative action establish acridine-based organotin complexes as promising anticancer candidates.

PMID:
42520359
Bibliographic data and abstract were imported from PubMed on 29 Jul 2026.

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