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Rhodium-catalyzed regio- and stereoselective β-C(sp2)-H amidation of enamines with dioxazolones to access vicinal diamines.

Created on 21 Aug 2026

Authors

Juan Chen, Huan Yuan, Yu-Xuan Ren, Xiao-Hui Cao, Shang-Shi Zhang, Bing Shu, Pengju Feng

Published in

Chemical communications (Cambridge, England). Aug 21, 2026. Epub Aug 21, 2026.

Abstract

Herein, a Rh(III)-catalyzed regio- and stereoselective β-C(sp2)-H amidation of enamides with dioxazolones has been developed, which afforded a series of diverse vicinal diamines with high Z-selectivity. This protocol featured mild conditions, broad substrate scope, and functional-group compatibility. In addition, scale-up synthesis, related applications, and preliminary mechanistic explorations were also accomplished.

PMID:
42627335
Bibliographic data and abstract were imported from PubMed on 21 Aug 2026.

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