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Chelation-Competition Interface Engineering of Polyphenol-Derived Coordination Polymers for Efficient Emulsion Separation.

Created on 06 Sep 2026

Authors

Rongtong Wang, Yijian Zheng, Yuanhang Pi, Chao Liang, Ying Jiang, Feipeng Jiao

Published in

Environmental research. Pages 125615. Sep 05, 2026. Epub Sep 05, 2026.

Abstract

Polyphenol-derived metal coordination polymers (MCPs) are promising for constructing hydrophilic and underwater antifouling membrane interfaces. However, conventional pH-regulated fabrication of MCPs is often accompanied by metal-ion hydrolysis, which consumes available metal ions and interferes with effective MCP formation. Herein, a triethanolamine (TEOA)-mediated chelation-competition strategy was developed to guide the in situ assembly of MCPs on separation membranes. TEOA modulated Fe3+ coordination and reactivity, while pre-adsorbed tannic acid (TA) subsequently displaced TEOA through competitive coordination to form Fe-TA MCPs. DFT calculations showed that the conversion from Fe-TEOA to Fe-polyphenol coordination was thermodynamically favorable (ΔG = -335.68 kJ/mol), supporting the proposed chelation-competition mechanism. The resulting FTC-PVDF exhibited superhydrophilicity, underwater superoleophobicity, and low oil adhesion. To leverage the low oil-droplet sliding angle, an inclined gravity-assisted cross-flow mode was further designed to facilitate oil-droplet migration and detachment. FTC-PVDF achieved a high permeance of 5300.5 L∙m-2∙h-1∙bar-1 and separation efficiencies above 99.5% for surfactant-stabilized emulsions. This work provides a chelation-competition interface-engineering route for regulating polyphenol-derived MCP formation and constructing high-permeance antifouling membranes for emulsion separation.

PMID:
42700856
Bibliographic data and abstract were imported from PubMed on 06 Sep 2026.

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